化工社化工社 化学情報印刷レポート · 研究参考用
1,3-Diisopropylbenzene → 1,3-Diisopropylbenzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,3-Diisopropylbenzene | HCID 7450 | — |
| 反応物 | Mycophenolic acid glucuronide | HCID 6442661 | — |
| 反応物 | m-Diisopropylbenzene monohydroperoxide | HCID 71436539 | — |
| 生成物 | 1,3-Diisopropylbenzene | HCID 7450 | — |
| 生成物 | Hydroperoxide,1,1'-[1,3-phenylenebis(1-methylethylidene)]bis- | HCID 53471113 | — |
| 生成物 | m-Diisopropylbenzene monohydroperoxide | HCID 71436539 | — |
反応手順
The raw material liquid for oxidation usually contains 20 to 60% by weight of m-diisopropylbenzene monohydroperoxide and 10 to 40% by weight of m-diisopropylbenzene. As usual reaction conditions, a temperature of 70 to 110° C., a pressure of 0 to 1 MPaG, a residence time of about 0.01 to 50 hours and the like are illustrated. As an apparatus used in the oxidation step, for example, a flowing type or batch type reaction vessel or reaction column can be listed. The oxidation reaction mixture obtained in the oxidation step usually contains 3 to 30% by weight of m-diisopropylbenzene dihydroperoxide and 20 to 60% by weight of m-diisopropylbenzene monohydroperoxide and 35% by weight or less of m-diisopropylbenzene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07488853B2 |
| 出典データセット | uspto-grants-2009_02 |
| ORD ID | ord-84d300448354445b89e57a2f3dfe2257 |
| 出典メモ | uspto-grants-2009_02 |