化工社化工社 化学情報印刷レポート · 研究参考用
Lactitol dihydrate → Lactulose
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lactitol dihydrate | HCID 157354 | — |
| 反応物 | Lactitol Monohydrate | HCID 3067270 | — |
| 生成物 | Lactulose | HCID 11333 | — |
反応手順
Examples XII-XXVII elucidate the conditions at which lactitol monohydrate and lactitol dihydrate, respectively, may be obtained from aqueous solutions of lactitol. In each instance 200 g lactitol dihydrate was used as the starting material which wasd dissolved in an amount of water varying from 40 g to 50 g at 100° C. Thereupon the solutions obtained were cooled to a temperature varying from 25° C. to 45° C. and seeded with 2 g monohydrate or 2 g dihydrate. The crystallization proper occurred at temperatures between 18° C. and 45° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05726303 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-3780dab8e7fc4abdb18faae656691afb |
| 出典メモ | uspto-grants-1998_03 |