Dicyclohexylcarbodiimide → 2-[4-(5-[propyloxy]-1-pentyl)phenyl]-5-([(Z)-3-octenoyl]oxy)pyridine
反応式
[C:1]([OH:10])(=[O:9])[CH2:2]/[CH:3]=[CH:4]\[CH2:5][CH2:6][CH2:7][CH3:8].[CH2:11]([O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]1[CH:25]=[CH:24][C:23]([C:26]2[CH:31]=[CH:30][C:29](O)=[CH:28][N:27]=2)=[CH:22][CH:21]=1)[CH2:12][CH3:13].C1(N=C=NC2CCCCC2)CCCCC1>ClCCl>[CH2:11]([O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]1[CH:21]=[CH:22][C:23]([C:26]2[CH:31]=[CH:30][C:29]([O:9][C:1](=[O:10])[CH2:2]/[CH:3]=[CH:4]\[CH2:5][CH2:6][CH2:7][CH3:8])=[CH:28][N:27]=2)=[CH:24][CH:25]=1)[CH2:12][CH3:13]参加物
5
実験手順
0.5 g of (Z)-3-octenoic acid, 1.0 g of 2-[4-(5-[propyloxy]-1-pentyl)phenyl]-5-hydroxypyridine, 07 g of N,N'-dicyclohexyl-carbodiimide, 0.04 g of (dimethylaminio)pyridine and 50 ml of dichloromethane were reacted in an analogous manner to Example 1 to give 2-[4-(5-[propyloxy]-1-pentyl)phenyl]-5-([(Z)-3-octenoyl]oxy)pyridine.