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Sodium Hydroxide → 2-Methylanthraquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Methyl-1,4-naphthoquinone sodium hydrogensulfite | HCID 23694936 | — |
| 生成物 | 2-Methylanthraquinone | HCID 6773 | — |
反応手順
A 0.5N aqueous sodium hydroxide solution was added to the oil phase obtained in Example 14, and, after 30 minutes stirring, air was blown thereinto at 70° C. for 2 hours. Then, the oil phase and the aqueous phase containing the precipitate were separated, and the aqueous phase was dried under reduced pressure to obtain 5.5 kg of 2-methylanthraquinone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05329026 |
| 出典データセット | uspto-grants-1994_07 |
| ORD ID | ord-8413aed7ab6d412189a9f71f8dc2eb86 |
| 出典メモ | uspto-grants-1994_07 |