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1-Phenylcyclohexane-1-carboxylic acid → Methyl 1-phenylcyclohexane-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Phenylcyclohexane-1-carboxylic acid | HCID 70817 | — |
| 反応物 | Methyl cyclopentanecarboxylate | HCID 78365 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | Methyl 1-phenylcyclohexane-1-carboxylate | HCID 15105202 | — |
反応手順
This compound was prepared (1.91 g, 8.76 mmol, 89%) from the product of Step A (2.00 g, 9.8 mmol) following the procedure for synthesis of methyl-1-cyclopentanecarboxylate as set forth in Step A, Example 1. The product of this step was homogeneous by TLC (ether:C2Cl2, 2:1) and used in the next step without further purification. CIMS 219 m/z (M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05331010 |
| 出典データセット | uspto-grants-1994_07 |
| ORD ID | ord-a3d1cba68a344dc4abd002d70273a898 |
| 出典メモ | uspto-grants-1994_07 |