化工社化工社 化学情報印刷レポート · 研究参考用
Ethylamine → 4-Ethylamino-3-nitrobenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylamine | HCID 6341 | — |
| 反応物 | 4-Chloro-3-nitrobenzamide | HCID 27942 | — |
| 生成物 | 4-Ethylamino-3-nitrobenzamide | HCID 3708922 | — |
反応手順
II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03989522 |
| 出典データセット | uspto-grants-1976_11 |
| ORD ID | ord-bb3097a7e15a44488e01fcb467723d81 |
| 出典メモ | uspto-grants-1976_11 |