Hydrochloric Acid → HCID 68138108、化合物

反応式

[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][NH:11][CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2.Cl[CH2:16][CH2:17][CH2:18][CH2:19][C:20]([NH2:22])=[O:21].Cl>>[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][N:11]([CH2:16][CH2:17][CH2:18][CH2:19][C:20]([NH2:22])=[O:21])[CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2

参加物

反応物 3

HCID 313Hydrochloric Acid

HCID 190471785-Chloropentanamide

HCID 214987881,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine

生成物 1

HCID 68138108HCID 68138108、化合物

実験手順

1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and 5-chlorovaleric acid amide are reacted in accordance with the process described in Example 1. Reaction period 19 hours at 60°. The hydrochloride of the title compound has a M.P. of 194°-196° from ethanol.

後処理

customReaction period 19 hours at 60°

出典と根拠

ORDレコード: ord-14abfcc78aaf4330ba9be99f05537801
出典データセット: uspto-grants-1976_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US03991066

反応ノート

読み込み中…