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Hydrochloric Acid → 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl)-N-phenylpropionic acid amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N-Phenylacrylamide | HCID 221792 | — |
| 反応物 | 1,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine | HCID 21498788 | — |
| 生成物 | 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl)-N-phenylpropionic acid amide | HCID 68139055 | — |
反応手順
1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and N-phenyl acrylamide are reacted in accordance with the process described in Example 6. Reaction period 4 hours. M.P. of the hydrochloride of the title compound 207°-209° from 95% ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03991066 |
| 出典データセット | uspto-grants-1976_11 |
| ORD ID | ord-dfd3edd2b6e24ecda950bbbca3bb4bba |
| 出典メモ | uspto-grants-1976_11 |