Hydrazine → 5-Trifluoromethyl-2-aminobenzophenone hydrazone

反応式

[F:1][C:2]([F:19])([F:18])[C:3]1[CH:4]=[CH:5][C:6]([NH2:17])=[C:7]([CH:16]=1)[C:8]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=O.[NH2:20][NH2:21]>>[F:1][C:2]([F:19])([F:18])[C:3]1[CH:4]=[CH:5][C:6]([NH2:17])=[C:7]([CH:16]=1)[C:8](=[N:20][NH2:21])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

参加物

反応物 2

HCID 9321Hydrazine

HCID 13014169(2-Amino-5-(trifluoromethyl)phenyl)(phenyl)methanone

生成物 1

HCID 867331125-Trifluoromethyl-2-aminobenzophenone hydrazone

実験手順

In the manner given in Preparation 1, 5-(trifluoromethyl)-2-aminobenzophenone is refluxed with hydrazine hydratein diethylene glycol to give 5-trifluoromethyl-2-aminobenzophenone hydrazone.

出典と根拠

ORDレコード: ord-99eca4f15604446fa30112c0fe46c96e
出典データセット: uspto-grants-1976_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US03992400

反応ノート

読み込み中…