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Ethylene Glycol → 1-(3-Pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylene Glycol | HCID 174 | — |
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | Diethyl Ether | HCID 3283 | — |
| 反応物 | Pyrinuron | HCID 40813 | — |
| 溶媒 | Dimethyl Ether | HCID 8254 | — |
| 生成物 | 1-(3-Pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide | HCID 20368872 | 76% |
反応手順
Gaseous HBr was passed into a solution of 3 g. of 3-pyridylmethyl-3-(4-nitrophenyl)urea in the monomethyl ether of ethyleneglycol. Ether was added to give a precipitate and after isolation, washing with ether and drying, 2.95 g. of white solid was obtained. This was a 76% yield of 1-(3-pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03994905 |
| 出典データセット | uspto-grants-1976_11 |
| ORD ID | ord-c90e0c80e13f467ab0012d87ee8db524 |
| 出典メモ | uspto-grants-1976_11 |