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1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane → 1-(2-Amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane | HCID 20165716 | — |
| 触媒 | Nickel | HCID 935 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 1-(2-Amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane | HCID 20165755 | — |
反応手順
1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane is dissolved in methanol and hydrogenated at 50 psi with Raney nickel T-1 as a catalyst. The reaction mixture is filtered through Celite and evaporated to yield 1-(2-amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04622418 |
| 出典データセット | uspto-grants-1986_11 |
| ORD ID | ord-d0aefeb1c0c4416a8c85c1796b9e05af |
| 出典メモ | uspto-grants-1986_11 |