化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → N,N-Dimethylaminopropyl acrylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 3-Hydroxypropanamide | HCID 4145140 | — |
| 生成物 | N,N-Dimethylaminopropyl acrylamide | HCID 77452 | — |
反応手順
59.3 g of β-hydroxypropionic acid amide and 68 g of 3-dimethylaminopropylamine were heated for 5 hours in a temperature range of 125°-168° C. until the evolution of ammonia was complete. After adding 1 g of pulverised sodium hydroxide the reaction mixture was distilled.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04237067 |
| 出典データセット | uspto-grants-1980_12 |
| ORD ID | ord-9fb2048b1977420aad17c78493b3ea51 |
| 出典メモ | uspto-grants-1980_12 |