化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → N,N-Dimethylaminopropyl acrylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | N-(3-dimethylaminopropyl)-3-methoxypropionamide | HCID 3097421 | — |
| 生成物 | N,N-Dimethylaminopropyl acrylamide | HCID 77452 | — |
反応手順
188.3 g (1.0 mole) of N-(3-dimethylaminopropyl)-3-methoxypropionamide (according to Example 13 ) are heated with 1.5 g of sodium hydroxide at 90°-110° C. in a high vacuum. Within about 30 minutes methanol is split off, vigorous forming occurring. The temperature is increased and 103 g (0.66 mole=66% of the theoretical yield) of colorless oil having a Bp0.1 of 96°-100° C. are distilled off.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04237067 |
| 出典データセット | uspto-grants-1980_12 |
| ORD ID | ord-69b2edd453b647a8857b466efd7201f5 |
| 出典メモ | uspto-grants-1980_12 |