化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → 2-Butylmercaptoaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Chloroacetyl chloride | HCID 6577 | — |
| 反応物 | o-Nitrobenzenethiol | HCID 21002 | — |
| 反応物 | 2-Pyrrolidinone, 1-(hydroxymethyl)- | HCID 84911 | — |
| 生成物 | 2-Butylmercaptoaniline | HCID 10329960 | — |
反応手順
2-Butylmercaptoaniline was prepared from -2-nitrothiophenol by a two-step reaction sequence consisting of alkylation followed by reduction corresponding to the procedure described in Example 4. The aniline then was condensed with N-methylolpyrrolidone, followed by reaction with chloroacetyl chloride to yield the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04239688 |
| 出典データセット | uspto-grants-1980_12 |
| ORD ID | ord-9bb7ea5ee3214d5ca67c785aa455bc90 |
| 出典メモ | uspto-grants-1980_12 |