Melamine → Melamine phosphate

HRID 1732874ノート

反応式

HRID 1732874 の反応式
[N:1]1[C:8]([NH2:9])=[N:7][C:5]([NH2:6])=[N:4][C:2]=1[NH2:3].[P:10]([OH:14])([O-:13])([O-:12])=[O:11].[NH4+].[NH4+]>>[P:10]([OH:14])([OH:13])([OH:12])=[O:11].[N:1]1[C:8]([NH2:9])=[N:7][C:5]([NH2:6])=[N:4][C:2]=1[NH2:3]

参加物

3

反応物 2

HCID 7955MelamineHCID 24540Diammonium hydrogen phosphate

生成物 1

HCID 92612Melamine phosphate

実験手順

Purified diammonium phosphate is produced by neutralizing relatively pure melamine orthophosphate, prepared from wet-process phosphoric acid, with ammonia in a hot solution of diammonium phosphate to give a slurry of melamine in concentrated diammonium phosphate solution. The liberated melamine is virtually insoluble in concentrated diammonium phosphate solutions; it is filtered from the hot mixture, washed, and recycled to produce more melamine phosphate by reaction with wet-process phosphoric acid. The hot, concentrated diammonium phosphate filtrate is cooled to precipitate purified diammonium phosphate crystals. The product is separated from its mother liquor by filtration, and the resulting filtrate is recycled to the reactor. The small amount of impurities introduced with the melamine phosphate are removed partly with the liberated melamine and partly by centrifugation of the diammonium phosphate solution. The only starting materials for the process are phosphoric acid and ammonia.

後処理

  1. filtrationit is filtered from the hot mixture
  2. washwashed

出典と根拠

ORDレコード
ord-1c02ea857b53403681663c8eaeda510b
出典データセット
uspto-grants-1980_12
特許番号
US04239739

反応ノート

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