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HRID 1733071作成日:2026年10月26日

19-Hydroxy-6alpha-methyl-4-androstene-3,17-dione → 1beta-Methyl-19-triphenylsiloxy-4-androstene-3,17-dione

https://huagongshe.com/reaction/1733071

反応式

関与物質

役割名称HCID仕込み量
反応物19-Hydroxy-6alpha-methyl-4-androstene-3,17-dioneHCID 70583925—
反応物19-(Triphenylsiloxy)-4-androstene-3,17-dione methanolateHCID 86735679—
生成物1beta-Methyl-19-triphenylsiloxy-4-androstene-3,17-dioneHCID 22803265—

反応手順

Following essentially the same procedure but substituting 19-hydroxhy-1β-methyl-4-androstene-3,17-dione and 19-hydroxy-6α-methyl-4-androstene-3,17-dione for the 19-hydroxy-4-androstene-3,17-dione above results in the preparation of 1β-methyl-19-triphenylsiloxy-4-androstene-3,17-dione and 6α-methyl-19-triphenylsilioxy-4-androstene-3,17-dione.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04239681
出典データセットuspto-grants-1980_12
ORD IDord-92dc09a3029d4cd5b7d6bda769053cc5
出典メモuspto-grants-1980_12