反応式
C1(C)C=CC=CC=1.[CH:8]([NH:11][C:12]1[N:17]=[C:16]([NH:18][CH:19]([CH3:21])[CH3:20])[N:15]=[C:14](P(OCC)(=O)OCC)[N:13]=1)([CH3:10])[CH3:9].[Cl:30]C(Cl)(Cl)C>O1CCOCC1>[Cl:30][C:14]1[N:13]=[C:12]([NH:11][CH:8]([CH3:10])[CH3:9])[N:17]=[C:16]([NH:18][CH:19]([CH3:21])[CH3:20])[N:15]=1参加物
5
実験手順
Similar reactions, in which 1,1,1-trichloroethane (reflux 75° C.) and 1,4-dioxan (reflux 105° C.) were used as solvents instead of toluene, both gave diethyl 2,4-bis(isopropylamino)-1,3,5-triazine-6-phosphonate in 81% yield, together with 2-chloro-4,6-bis(isopropylamino)-1,3,5-triazine (yield 12-17%).
出典と根拠
- ORDレコード
- ord-e3aaf468c36b4760b98f8dcc8acce084
- 出典データセット
- uspto-grants-1996_07
- 特許番号
- US05534573
関連ノート
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