化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → 1,3-Bis(2-t-amylperoxy-2-propyl)benzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | p-Bis(2-hydroxyisopropyl)benzene | HCID 18062 | — |
| 反応物 | tert-Amyl hydroperoxide | HCID 76962 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 1,3-Bis(2-t-amylperoxy-2-propyl)benzene | HCID 54131583 | — |
反応手順
1,4-Bis(2-t-amylperoxy-2-propyl)benzene (para III) was prepared by reacting 28.1 grams (0.231 mole) of aqueous 85.7% t-amyl hydroperoxide diluted with 3.2 grams of water with 20.4 grams (0.105 mole) of 1,4-bis(2-hydroxy-2-propyl)benzene in the presence of 44.1 grams (0.316 mole) of 70% sulfuric acid according to the procedure of Example VII. The stripped product was a yellow liquid which remained liquid at 15° C. The product weighed 32.0 grams.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05539061 |
| 出典データセット | uspto-grants-1996_07 |
| ORD ID | ord-4a4d45c4eb9243e2a9facd98ed10c5f3 |
| 出典メモ | uspto-grants-1996_07 |