Carbon Dioxide → HCID 54358079、化合物

HRID 1735947ノート

反応式

HRID 1735947 の反応式
[CH2:1]([O:3][C:4](=[O:37])[C:5](=[NH:36])[CH:6](P(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)[CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH3:2].[C:38](=O)=[O:39]>>[CH2:1]([O:3][C:4](=[O:37])[CH:5]([N:36]=[C:38]=[O:39])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:14])([CH3:15])[CH3:16])=[O:11])[CH3:2]

参加物

3

反応物 2

HCID 280Carbon DioxideHCID 178472716HCID 178472716、化合物

生成物 1

HCID 54358079HCID 54358079、化合物

反応条件

温度
50 °C

実験手順

The reaction solution from Example 9 is placed in a Parr® bomb and carbon dioxide (22 g, 0.5 mol) is condensed into the bomb. The bomb is sealed and heated to 50° C. for 12 hours. The bomb is cooled and vented to atmospheric pressure. The solution is transferred from the bomb to a flask and used as is in the next reaction (Example 11).

後処理

  1. customcondensed into the bomb
  2. customThe bomb is sealed
  3. temperatureThe bomb is cooled
  4. customThe solution is transferred from the bomb to a flask
  5. customas is in the next reaction (Example 11)

出典と根拠

ORDレコード
ord-faeadfd5a0604f41986fed3e3c12fa5d
出典データセット
uspto-grants-1996_07
特許番号
US05539082

反応ノート

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