化工社化工社 化学情報印刷レポート · 研究参考用
1-Phenylpiperazine → alpha-{[1-(4-Phenylpiperazinyl)]methyl}benzeneacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Phenylpiperazine | HCID 7096 | — |
| 反応物 | Atropic acid | HCID 68114 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | alpha-{[1-(4-Phenylpiperazinyl)]methyl}benzeneacetic acid | HCID 19433570 | — |
反応手順
1-Phenylpiperazine and atropic acid in ethanol is heated under reflux for 18 h, cooled to room temperature, and evaporated in vacuo. The solid is triturated with acetone to give the title product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05541326 |
| 出典データセット | uspto-grants-1996_07 |
| ORD ID | ord-c01c36e3f54a425eb1d7bffdd9f68b80 |
| 出典メモ | uspto-grants-1996_07 |