1,2,3,6-Tetrahydro-1-methylpyridine-4-methanol → 1-Acetyl-8bromo-7-(1-methyl-1,2,3,6-tetrahydro-4-pyridyl)methoxy-2,3,4,5-tetrahydro-1H-benzazepine
反応式
[C:1]([N:4]1[C:10]2[CH:11]=[C:12]([Br:16])[C:13]([OH:15])=[CH:14][C:9]=2[CH2:8][CH2:7][CH2:6][CH2:5]1)(=[O:3])[CH3:2].O[CH2:18][C:19]1[CH2:20][CH2:21][N:22]([CH3:25])[CH2:23][CH:24]=1>>[C:1]([N:4]1[C:10]2[CH:11]=[C:12]([Br:16])[C:13]([O:15][CH2:18][C:19]3[CH2:24][CH2:23][N:22]([CH3:25])[CH2:21][CH:20]=3)=[CH:14][C:9]=2[CH2:8][CH2:7][CH2:6][CH2:5]1)(=[O:3])[CH3:2]参加物
3
実験手順
The title compound was prepared from 1-acetyl-8-bromo-7-hydroxy-2,3,4,5-tetrahydro-1H-benzazepine (D25) and 4-(hydroxymethyl)-1-methyl-1,2,3,6-tetrahydropyridine (D1) following the procedure of Description 2.
出典と根拠
- ORDレコード
- ord-b07d0eedd89a492c9b5f43be722ebfe3
- 出典データセット
- uspto-grants-1999_10
- 特許番号
- US05972951
反応ノート
読み込み中…