2-Chloro-N,N-dimethylethylamine → HCID 9803568、化合物

反応式

[CH3:1][N:2]([CH2:4][CH2:5]Cl)[CH3:3].[CH3:7][O:8][C:9]1[CH:14]=[CH:13][C:12]([C:15]2[O:16][C:17]3[CH:32]=[C:31]([O:33][CH3:34])[CH:30]=[CH:29][C:18]=3[C:19]=2[C:20](=[O:28])[C:21]2[CH:26]=[CH:25][C:24]([OH:27])=[CH:23][CH:22]=2)=[CH:11][CH:10]=1>>[CH3:7][O:8][C:9]1[CH:14]=[CH:13][C:12]([C:15]2[O:16][C:17]3[CH:32]=[C:31]([O:33][CH3:34])[CH:30]=[CH:29][C:18]=3[C:19]=2[C:20](=[O:28])[C:21]2[CH:26]=[CH:25][C:24]([O:27][CH2:5][CH2:4][N:2]([CH3:3])[CH3:1])=[CH:23][CH:22]=2)=[CH:11][CH:10]=1

参加物

反応物 2

HCID 79012-Chloro-N,N-dimethylethylamine

HCID 10044927HCID 10044927、化合物

生成物 1

HCID 9803568HCID 9803568、化合物

実験手順

The title compound was prepared essentially as described in Example 24, supra, except that 2-(N,N-dimethylamino)ethyl chloride was reacted with 2-(4-methoxyphenyl)-3-(4-hydroxybenzoyl)-6-methoxybenzofuran instead of the 2-(N,N-diisopropylamino)ethyl chloride employed in that example.

出典と根拠

ORDレコード: ord-f7297971224443909ee6eef0ed8cbcdc
出典データセット: uspto-grants-1999_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05972888

反応ノート

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