化工社化工社 化学情報印刷レポート · 研究参考用
Tert-butyl 2-nitro-4-thien-3-ylphenylcarbamate → Tert-butyl [2-amino-4-(3-thienyl)phenyl]carbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tert-butyl 2-nitro-4-thien-3-ylphenylcarbamate | HCID 66865115 | — |
| 触媒 | Nickel | HCID 935 | — |
| 生成物 | Tert-butyl [2-amino-4-(3-thienyl)phenyl]carbamate | HCID 57717476 | — |
反応手順
Prepared from (2-nitro-4-thiophen-3-yl-phenyl)-carbamic acid tert.-butyl ester (Example B2) by catalytic hydrogenation with Raney-Ni according to the general procedure G (method a). Obtained as a white solid (278 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07018998B2 |
| 出典データセット | uspto-grants-2006_03 |
| ORD ID | ord-b522c29a4c5440afa1f96caff081ea3d |
| 出典メモ | uspto-grants-2006_03 |