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N-Isopropylpropylamine → N-[4-(aminosulfonyl)-2-methylphenyl]-6-[isopropyl(propyl)amino]pyrimidine-4-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Isopropylpropylamine | HCID 89119 | — |
| 反応物 | 6-Chloro-pyrimidine-4-carboxylic acid (2-methyl-4-sulfamoyl-phenyl)amide | HCID 59447056 | — |
| 生成物 | N-[4-(aminosulfonyl)-2-methylphenyl]-6-[isopropyl(propyl)amino]pyrimidine-4-carboxamide | HCID 25182908 | — |
反応手順
Following the general method as outlined in Example 20, starting from 6-chloro-pyrimidine-4-carboxylic acid (2-methyl-4-sulfamoyl-phenyl)-amide (Intermediate 17) and propyl-isopropylamine (Matrix), the title compound was obtained as a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09150519B2 |
| 出典データセット | uspto-grants-2015_10 |
| ORD ID | ord-ebefd2436549403aa7d66edf0dcd526a |
| 出典メモ | uspto-grants-2015_10 |