反応式
[OH:1][CH2:2][C:3]1[N:8]=[C:7]([C:9](=O)[CH3:10])[CH:6]=[CH:5][CH:4]=1.[NH2:12][OH:13]>C(O)C>[OH:1][CH2:2][C:3]1[N:8]=[C:7]([C:9](=[N:12][OH:13])[CH3:10])[CH:6]=[CH:5][CH:4]=1参加物
4
実験手順
To a solution of 1643 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone in 25 ml of ethanol was added 0.72 ml of a 50% aqueous hydroxylamine solution, followed by stirring overnight. The reaction solution was concentrated under reduced pressure to obtain 1806 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone oxime as an amorphous substance.
後処理
- concentrationThe reaction solution was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-cbce93e8394845eaade63b03730db94c
- 出典データセット
- uspto-grants-2015_10
- 特許番号
- US09150541B2
関連ノート
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