Chlorosuccinimide → N-Hydroxy-4,4-dimethylcyclohexanecarbimidoyl chloride

反応式

[CH3:1][C:2]1([CH3:11])[CH2:7][CH2:6][CH:5]([CH:8]=[N:9][OH:10])[CH2:4][CH2:3]1.[Cl:12]N1C(=O)CCC1=O>>[OH:10][N:9]=[C:8]([Cl:12])[CH:5]1[CH2:4][CH2:3][C:2]([CH3:11])([CH3:1])[CH2:7][CH2:6]1

参加物

反応物 2

HCID 31398Chlorosuccinimide

HCID 86704401HCID 86704401、化合物

生成物 1

HCID 86704402N-Hydroxy-4,4-dimethylcyclohexanecarbimidoyl chloride

実験手順

N-Hydroxy-4,4-dimethylcyclohexanecarbimidoyl chloride (I-9D) was prepared by reaction of 4,4-dimethylcyclohexanecarbaldehyde oxime and N-chloro succinimide following the same protocol as described for I-6B. MS m/z 190.1 (M+1).

出典と根拠

ORDレコード: ord-b751ef8d0ea449a8b916eeead431776d
出典データセット: uspto-grants-2015_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US09150568B2

反応ノート

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