2-Amino-1,2-diphenylethanol → HCID 58080370、化合物
反応式
[N:1]1([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH2:6][CH2:5][CH:4]([C:7]([O-:9])=O)[CH2:3][CH2:2]1.[NH2:17][CH:18]([C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)[CH:19]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)O>>[C:27]1([C:18]2[N:17]=[C:7]([CH:4]3[CH2:3][CH2:2][N:1]([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH2:6][CH2:5]3)[O:9][C:19]=2[C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=1参加物
3
実験手順
Starting from 1.08 g of mono-tert-butyl piperidine-1,4-dicarboxylate and 1 g 2-amino-1,2-diphenyl-ethanol the product may be prepared as described in the literature (cf. Tet. 2001, 4867). The product is purified by chromatography (method B). 560 mg are obtained in the form of an oil. Analytical HPLC-MS (method A): RT=1.72 min.
後処理
- custommay be prepared
- customThe product is purified by chromatography (method B)
- custom560 mg are obtained in the form of an oil
出典と根拠
- ORDレコード
- ord-4d5a96054dfc41b4ab538d5659f3bea7