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HRID 1754020作成日:2026年10月25日

2-Nitrotoluene → Azoxybenzene

https://huagongshe.com/reaction/1754020

反応式

関与物質

役割名称HCID仕込み量
反応物2-NitrotolueneHCID 6944—
反応物NitrobenzeneHCID 7416—
反応物1-Ethyl-2-nitrobenzeneHCID 69156—
生成物AzoxybenzeneHCID 10316—

反応手順

The reduction reaction was carried out in the same manner as set forth in Example 6 except for using a mixture of 1.0 mmol of o-methyl nitrobenzene and 1.0 mmol of o-ethyl nitrobenzene instead of using nitrobenzene alone, and using 19.5 mg (the amount required for swelling of the reactant in 100%) of Polymer supported reagent-2, and thereby an azoxybenzene derivative of a symmetrical structure and an azoxybenzene derivative of an asymmetrical structure were obtained as a main product, respectively.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09169200B2
出典データセットuspto-grants-2015_10
ORD IDord-5640dc0bf2034804ae5f5c51180f0889
出典メモuspto-grants-2015_10