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Triglycidylglycerol → 1,2,3-Tris[3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)-2-hydroxypropoxy]propane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triglycidylglycerol | HCID 25795 | — |
| 反応物 | 2,2,6,6-Tetramethyl-4-piperidyl benzoate | HCID 579967 | — |
| 生成物 | 1,2,3-Tris[3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)-2-hydroxypropoxy]propane | HCID 20510591 | — |
反応手順
A mixture of 10.1 g of 4-benzoyloxy-2,2,6,6-tetramethylpiperidine and 2.6 g of glycerol tris(2,3-epoxypropyl)ether was reacted following the procedure described in Example 5 to give the desired Compound No. 115 in the form of a white vitreous solid having an Rf value of 0.87 on thin-layer chromatography on silica gel developed with a 4:1 by volume mixture of ethyl acetate and triethylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04371644 |
| 出典データセット | uspto-grants-1983_02 |
| ORD ID | ord-18a88326651540f8aad31d676b6135b5 |
| 出典メモ | uspto-grants-1983_02 |