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HRID 1758191作成日:2026年10月26日

Triglycidylglycerol → 1,2,3-Tris[3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)-2-hydroxypropoxy]propane

https://huagongshe.com/reaction/1758191

反応式

関与物質

役割名称HCID仕込み量
反応物TriglycidylglycerolHCID 25795—
反応物2,2,6,6-Tetramethyl-4-piperidyl benzoateHCID 579967—
生成物1,2,3-Tris[3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)-2-hydroxypropoxy]propaneHCID 20510591—

反応手順

A mixture of 10.1 g of 4-benzoyloxy-2,2,6,6-tetramethylpiperidine and 2.6 g of glycerol tris(2,3-epoxypropyl)ether was reacted following the procedure described in Example 5 to give the desired Compound No. 115 in the form of a white vitreous solid having an Rf value of 0.87 on thin-layer chromatography on silica gel developed with a 4:1 by volume mixture of ethyl acetate and triethylamine.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04371644
出典データセットuspto-grants-1983_02
ORD IDord-18a88326651540f8aad31d676b6135b5
出典メモuspto-grants-1983_02