化工社化工社 化学情報印刷レポート · 研究参考用
Ethanolamine → 2-[(1,1-Dioxidotetrahydro-3-thienyl)amino]ethanol hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanolamine | HCID 700 | — |
| 反応物 | 3-Aminotetrahydrothiopene 1,1-dioxide hydrochloride | HCID 2795201 | — |
| 生成物 | 2-[(1,1-Dioxidotetrahydro-3-thienyl)amino]ethanol hydrochloride | HCID 16896370 | — |
反応手順
The procedure of Example 1 was repeated substituting 95 percent monoethanolamine (28.6 parts) for the ammonium hydroxide of Example 1. A sticky solid was filtered after treatment with hydrochloric acid, and upon drying in vacuo over P2O5 weighed 59.6 g. (78.5 percent of theory) m.p. 122°-124° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04374040 |
| 出典データセット | uspto-grants-1983_02 |
| ORD ID | ord-86cb4db8a7b940b4a64ef7d396ff5961 |
| 出典メモ | uspto-grants-1983_02 |