関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Boron trifluoride etherate | HCID 8000 | — |
| 反応物 | Methyl cumyl ether | HCID 70289 | — |
| 反応物 | Cumen hydroperoxide | HCID 53627471 | — |
| 生成物 | Dicumyl peroxide | HCID 6641 | 99.8% |
反応手順
There are loaded into a 100 ml glass flask, 30 grams of methyl cumyl ether (0.2 moles), 0.1 ml of boron trifluoride diethyl etherate and 9 grams of technical cumene hydroperoxide (0.05 moles) having the same composition as that used in Example 1. The mixture is heated to 60° C. with stirring and maintained at a pressure of 200 mmHg. After 30 minutes the conversion of the cumene hydroperoxide is 100% with a yield of 99.8% of dicumyl peroxide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04374279 |
|---|
| 出典データセット | uspto-grants-1983_02 |
|---|
| ORD ID | ord-d44841cc6a594b178f67f248c9e41fbc |
|---|
| 出典メモ | uspto-grants-1983_02 |
|---|
