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(2-((Dimethylamino)methyl)thiazol-4-yl)methanol → HCID 178482517、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (2-((Dimethylamino)methyl)thiazol-4-yl)methanol | HCID 1838020 | — |
| 反応物 | HCID 178482512 | HCID 178482512 | — |
| 溶媒 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | HCID 178482517 | HCID 178482517 | — |
反応手順
Reaction of 3-methylamino-4-(2-mercaptoethylamino)-1,2,5-thiadiazole 1,1-dioxide [prepared in Example 25, Step A] with about one equivalent of 2-dimethylaminomethyl-4-hydroxymethylthiazole [prepared in Example 34, Step D] in concentrated hydrochloric acid, and then made basic and worked up, produces the title compound which is identical to the product prepared in Example 33.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04374248 |
| 出典データセット | uspto-grants-1983_02 |
| ORD ID | ord-8b67ff6647a0405396011910233436e5 |
| 出典メモ | uspto-grants-1983_02 |