化工社化工社 化学情報印刷レポート · 研究参考用
Santonox → N-(1-methylethyl)-3-(3-methoxyphenyl)-2-oxiranecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Santonox | HCID 7308 | — |
| 反応物 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 反応物 | N-(1-methylethyl)-3-methoxycinnamoylcarboxamide | HCID 54220101 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | N-(1-methylethyl)-3-(3-methoxyphenyl)-2-oxiranecarboxamide | HCID 20490547 | — |
反応手順
This compound was prepared from N-(1-methylethyl)-3-methoxycinnamoylcarboxamide (43.9 g.), m-chloroperbenzoic acid (46 g.), 4,4'-thiobis(6-tert-butyl-m-cresol) (0.6 g.), and ethylene dichloride (500 ml.) as described in Example 7. The compound obtained as an oil was used directly in the subsequent reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04341718 |
| 出典データセット | uspto-grants-1982_07 |
| ORD ID | ord-52273c1409cf476cafcc5281fecb1265 |
| 出典メモ | uspto-grants-1982_07 |