4-Fluorobenzaldehyde → HCID 22600056、化合物
反応式
[CH3:1][S:2]([C:4]1[CH:10]=[CH:9][C:7]([NH2:8])=[CH:6][CH:5]=1)=[O:3].[F:11][C:12]1[CH:19]=[CH:18][C:15]([CH:16]=O)=[CH:14][CH:13]=1>C1C=CC=CC=1>[F:11][C:12]1[CH:19]=[CH:18][C:15]([CH:16]=[N:8][C:7]2[CH:9]=[CH:10][C:4]([S:2]([CH3:1])=[O:3])=[CH:5][CH:6]=2)=[CH:14][CH:13]=1参加物
4
実験手順
A mixture of 3.0 g (19 mmol) of 4-methylsulfinylaniline (obtained in reference example 3), 2 mL (19 mmol) of 4-fluorobenzaldehyde and 80 mL of benzene was refluxed in a Dean-Stark for 2 days. The solvent was removed and the crude product obtained was directly used in the next reaction.
後処理
- temperaturewas refluxed in a Dean-Stark for 2 days
- customThe solvent was removed
出典と根拠
- ORDレコード
- ord-4f6bba6e08f140aaba54235952f89967
- 出典データセット
- uspto-grants-2005_01
- 特許番号
- US06838476B1
反応ノート
読み込み中…