化工社化工社 化学情報印刷レポート · 研究参考用
4-Nitrobenzoyl chloride → Bis-(4-nitrobenzoyl)-tripropylene glycol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| 反応物 | 2-(2-(2-Hydroxypropoxy)propoxy)-1-propanol | HCID 32611 | — |
| 生成物 | Bis-(4-nitrobenzoyl)-tripropylene glycol | HCID 86743032 | 89% |
反応手順
Tripropylene glycol (57.6 g, 0.3 mole) was treated with p-nitrobenzoyl chloride (116 g, 0.625 mole), following the general procedure described in Example 1, Part A. The product, bis-(4-nitrobenzoyl)-tripropylene glycol (131 g), was obtained as a viscous yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04829099 |
| 出典データセット | uspto-grants-1989_05 |
| ORD ID | ord-3a748d601ca04ed6bc5cb8b5044b74cd |
| 出典メモ | uspto-grants-1989_05 |