Potassium Carbonate → HCID 19858315、化合物

HRID 1762129ノート

反応式

HRID 1762129 の反応式
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

参加物

5

反応物 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

生成物 1

HCID 19858315HCID 19858315、化合物

試薬・触媒・溶媒 1

HCID 24813Phosphorus oxychloride触媒

実験手順

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and was concentrated to obtain the product as an oil.

後処理

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationwas concentrated

出典と根拠

ORDレコード
ord-42518c203af64540aaafefcd08cba9c2
出典データセット
uspto-grants-1989_05
特許番号
US04831035

反応ノート

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