Acetic-formic anhydride → 2-Formamido-6-methylbenzyl alcohol
反応式
[CH:1](OC(=O)C)=[O:2].[NH2:7][C:8]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:9]=1[CH2:10][OH:11]>C1C=CC=CC=1.CCCCCC>[CH:1]([NH:7][C:8]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:9]=1[CH2:10][OH:11])=[O:2]参加物
5
実験手順
Acetic formic anhydride (1.85 g) was added to a solution of 2-amino-6-methylbenzyl alcohol (2.74 g) in benzene (55 ml) at room temperature. After being stirred for 2 hours, the mixture was diluted with n-hexane (10 ml) and the precipitates were collected by filtration to give 2-formamido-6-methylbenzyl alcohol (2.8 g).
後処理
- filtrationthe precipitates were collected by filtration
出典と根拠
- ORDレコード
- ord-31200514c4f54d2a9954e0aaa3bb2148
- 出典データセット
- uspto-grants-1989_05
- 特許番号
- US04831041
反応ノート
読み込み中…