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Sulfamide → HCID 178479209、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfamide | HCID 82267 | — |
| 反応物 | 3-Chloropropionitrile hydrogen chloride | HCID 86742043 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | HCID 178479209 | HCID 178479209 | — |
反応手順
To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04835281 |
| 出典データセット | uspto-grants-1989_05 |
| ORD ID | ord-6ec711e95d084ee185c242200ab7ae81 |
| 出典メモ | uspto-grants-1989_05 |