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Hydrochloric Acid → N-methyl-N-tert.-octylthiomethylamine hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 1,3,5-Trimethyl-1,3,5-triazacyclohexane | HCID 7952 | — |
| 反応物 | Tert.-octylthiomethylamine | HCID 86735983 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | N-methyl-N-tert.-octylthiomethylamine hydrochloride | HCID 85866484 | — |
反応手順
300 ml. of acetonitrile, 12.9 g. (0.1 mole) of 1,3,5-trimethylhexahydro-s-triazine; 43.8 g. (0.3 mole) of tert.-octylthiomethylamine and 12 g. of hydrogen chloride gas are reacted together in the manner of Example I. A yield of 43.7 g. (64.6% of theory) of the title compound is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04111682 |
| 出典データセット | uspto-grants-1978_09 |
| ORD ID | ord-dba2278fae3647809136087c4a36efe9 |
| 出典メモ | uspto-grants-1978_09 |