化工社化工社 化学情報印刷レポート · 研究参考用
Dimethyl Sulfide → (2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl Sulfide | HCID 1068 | — |
| 反応物 | Ethyl bromoacetate | HCID 7748 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | (2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide | HCID 78861 | — |
反応手順
A solution of ethyl bromoacetate (265 g) and dimethyl sulfide (114 g) in acetone (500 mL) was stirred at room temperature. After three days, the title compound was isolated by filtration of the reaction mixture. Melting point 88°-90° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05726320 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-d735999e237040e79efd9e34aa9e36bf |
| 出典メモ | uspto-grants-1998_03 |