2,4,5-Trichlorobenzenesulfonyl chloride → 2,4,5-Trichlorobenzenesulfonyl fluoride
反応式
[F-:1].[K+].[Cl:3][C:4]1[CH:9]=[C:8]([Cl:10])[C:7]([Cl:11])=[CH:6][C:5]=1[S:12](Cl)(=[O:14])=[O:13]>>[Cl:3][C:4]1[CH:9]=[C:8]([Cl:10])[C:7]([Cl:11])=[CH:6][C:5]=1[S:12]([F:1])(=[O:14])=[O:13]参加物
3
実験手順
2,4,5-Trichlorobenzenesulfonyl fluoride was synthesized from potassium fluoride and 2,4,5-trichlorobenzenesulfonyl chloride using the procedure described in Example 1. A product with mp 80°-83° C was obtained in 99% yield. The chemical analysis, NMR and IR spectra were in agreement with the assigned structure.
後処理
- customA product with mp 80°-83° C was obtained in 99% yield
出典と根拠
- ORDレコード
- ord-c6cc9c6cc38b44a593ddd35998180d7c
- 出典データセット
- uspto-grants-1978_09
- 特許番号
- US04115059
反応ノート
読み込み中…