2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chlorophenyl)-4-tert-butylbenzenesulfonamide

関与物質

反応手順

The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 115 mg of (2-amino-5-chloro-phenyl)-phenyl-methanone and 116 mg of 4-tert-Butyl-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 1.21 (s, 9H), 7.28–7.34 (m, 3H), 7.37–7.44 (m, 4H), 7.48 (dd, 1H, J=8.8, 2.4 Hz), 7.54–7.62 (m, 3H), 7.78 (d, 1H, J=8.8 Hz), 9.89 (s, 1H). MS: m/z 428.9 (M++1).

情報源と証拠