化工社化工社 化学情報印刷レポート · 研究参考用
2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chloro-phenyl)-3-cyano-benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| 反応物 | 3-Cyanobenzene-1-sulfonyl chloride | HCID 2801360 | — |
| 生成物 | N-(2-benzoyl-4-chloro-phenyl)-3-cyano-benzenesulfonamide | HCID 11211650 | — |
反応手順
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using (2-amino-5-chloro-phenyl)-phenyl-methanone and 3-Cyano-benzenesulfonyl chloride. 1H NMR (CDCl3): δ 7.39–7.45 (m, 6H), 7.53–7.62 (m, 3H), 7.43 (d, J=8.4 Hz, 1H), 7.91 (bs, 2H), 9.77 (s, 1H). MS: m/z 396.9 (M++1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07227035B2 |
| 出典データセット | uspto-grants-2007_06 |
| ORD ID | ord-e1a91142dd9440d1a02238c47ad950c4 |
| 出典メモ | uspto-grants-2007_06 |