関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 3-Nitrophenol | HCID 11137 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Methanesulfonate | HCID 85257 | — |
| 反応物 | Diethylamino-propanol | HCID 5256659 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | N,N-diethyl-N-[3-(3-nitrophenoxy)propyl]amine | HCID 22012884 | — |
反応手順
To a stirred solution of 3-nitrophenol (2 mmol) in DMF (6 mL) at rt, solid potassium carbonate (4 mmol) was added. A solution of the mesylate of N,N-diethylaminopropanol (2.2 mmol) in DMF (2 mL) was then added to the reaction mixture and heated to 80° C. until completion, according to General Procedure Q1, as indicated by TLC or HPLC. After cooling to rt, the reaction mixture was then treated with cold H2O (15 mL), and extracted with EtOAc (2×15 mL). The combined organic layers were washed with brine and dried over sodium sulfate. Evaporation of the solvent in vacuuo afforded the desired N,N-diethyl-N-[3-(3-nitrophenoxy)propyl]amine. The crude product was used directly for further transformation.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US07737285B2 |
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| 出典データセット | uspto-grants-2010_06 |
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| ORD ID | ord-1a59dbac1df94d85990d11a3d8f7174d |
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| 出典メモ | uspto-grants-2010_06 |
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