1-Iodo-4-propylbenzene → HCID 178506682、化合物
反応式
[CH2:1]([C:4]1[CH:9]=[CH:8][C:7](I)=[CH:6][CH:5]=1)[CH2:2][CH3:3].C([Li:15])CCC>CCCCCC>[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[Li:15])[CH2:2][CH3:3]参加物
4
実験手順
Air in a dried four-necked flask was replaced with nitrogen, and 10 ml of n-hexane and 2.86 g (0.0116 mol) of p-n-propyliodobenzene were introduced. Then, 10 ml of a hexane solution of n-butyl lithium (0.0116 mol) was gradually added thereto under stirring to obtain a hexane solution of n-propylphenyl lithium.
後処理
- additionwere introduced
出典と根拠
- ORDレコード
- ord-4b190226ff2742a6b1d07963b1a1915f
- 出典データセット
- uspto-grants-1995_01
- 特許番号
- US05380461
反応ノート
読み込み中…