6-Amino-1-hexanol → HCID 178459129、化合物

HRID 1769588ノート

反応式

HRID 1769588 の反応式
[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[Ti+3:13].[NH2:14]CCCCCCO>>[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[NH2:14][Ti+3:13][CH2:1][CH2:2][CH2:4][CH2:5][CH2:6][CH3:8]

参加物

3

反応物 2

HCID 199606-Amino-1-hexanolHCID 9815954Titanium(3+) propan-2-olate

生成物 1

HCID 178459129HCID 178459129、化合物収率 200%

実験手順

0.1 moles of titanium-tri-isopropoxide (Tyzor TPT Dupont, Wilmington, Del.) and 0.1 moles of 6-amino-1-hexanol were added to a 50 ml beaker and stirred at room temperature for 1 minute to form 0.1 mole of amino-hexyl-titanium-tri-isopropoxide. The reaction mixture was heated to 70° C. for 10 minutes to evaporate the isopropyl alcohol formed during the reaction.

出典と根拠

ORDレコード
ord-67ab2309cf784c37b94831901886f134
出典データセット
uspto-grants-1995_01
特許番号
US05382468

反応ノート

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