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4-Benzeneazodiphenylamine → Aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Benzeneazodiphenylamine | HCID 7575 | — |
| 反応物 | Cyclohexanol | HCID 7966 | — |
| 反応物 | Potassium tert-butoxide | HCID 23665647 | — |
| 生成物 | Aniline | HCID 6115 | — |
| 生成物 | N-Phenyl-p-phenylenediamine | HCID 7564 | — |
反応手順
A solution of 4-(phenylazo)diphenylamine (0.273 g), cyclohexanol (5 g) and potassium t-butoxide (1 g) was heated at reflux under nitrogen for 4 hours. Analysis of the reaction mixture by HPLC indicated all of the 4-(phenyazo)-diphenylamine was consumed. 4-aminodiphenylamine and aniline were produced in 99% yield based on 4-(phenylazo)diphenylamine charged.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05382691 |
| 出典データセット | uspto-grants-1995_01 |
| ORD ID | ord-c8e6b65f71374bab982a36394e8cf5ba |
| 出典メモ | uspto-grants-1995_01 |