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Pyrimidine, 2,4-dichloro-5-methyl- → 2-Chloro-5-methyl-N4-(4-methyl-3-oxo-benzo[1,4]thiazin-6-yl)-4-pyrimidineamine

HRID 1770846
ノート
印刷プレビュー

反応式

HRID 1770846 の反応式
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]2[S:10][CH2:9][C:8](=[O:11])[N:7]([CH3:12])[C:6]=2[CH:13]=1.[Cl:14][C:15]1[N:20]=[C:19](Cl)[C:18]([CH3:22])=[CH:17][N:16]=1>CO>[Cl:14][C:15]1[N:20]=[C:19]([NH:1][C:2]2[CH:3]=[CH:4][C:5]3[S:10][CH2:9][C:8](=[O:11])[N:7]([CH3:12])[C:6]=3[CH:13]=2)[C:18]([CH3:22])=[CH:17][N:16]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

4

反応物 2

HCID 74508Pyrimidine, 2,4-dichloro-5-methyl-HCID 219881476-Amino-4-methyl-2H-1,4-benzothiazin-3(4H)-one

生成物 1

HCID 866097232-Chloro-5-methyl-N4-(4-methyl-3-oxo-benzo[1,4]thiazin-6-yl)-4-pyrimidineamine収率 30.7%

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

A mixture of 1.3 g of 6-Amino-4-methyl-3-oxo-benzo[1,4]thiazine and 3.3 g of 2,4-Dichloro-5-methylpyrimidine in 100 mL methanol was stirred at RT overnight and was reduced in volume by rotary evaporation. The solution was filtered and the filtrate diluted with water and neutralized with sodium bicarbonate. The precipitate was collected by suction filtration washed with water and dried on the funnel to yield 660 mg 13% of the desired product 2-Chloro-5-methyl-N4-(4-methyl-3-oxo-benzo[1,4]thiazin-6-yl)-4-pyrimidineamine 1H NMR (DMSO-d6): δ 8.93 (s, 1H), 8.06 (m, 2H), 7.62 (s, 1H), 7.37 (s, 1H), 3.51 (s, 2H), 2.16 (s, 3H) purity 97%; MS (m/e) 321 (MH+).

後処理

  1. customwas reduced in volume by rotary evaporation
  2. filtrationThe solution was filtered
  3. additionthe filtrate diluted with water and neutralized with sodium bicarbonate
  4. filtrationThe precipitate was collected by suction filtration
  5. washwashed with water
  6. customdried on the funnel

出典と根拠

ORDレコード
ord-5be4699250834d1e924219ed630d810d
出典データセット
uspto-grants-2016_02
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US09248190B2

反応ノート

読み込み中…

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