Potassium Hydroxide → 1,1,1,2,3-Pentafluoropropane
反応式
[OH-].[K+].[CH2:3]([F:10])[CH:4]([F:9])[C:5]([F:8])([F:7])[F:6]>O>[CH2:3]([F:10])[CH:4]([F:9])[C:5]([F:8])([F:7])[F:6].[CH2:3]=[C:4]([F:9])[C:5]([F:8])([F:7])[F:6]参加物
5
反応条件
- 温度
- 160 °C
実験手順
Use is made of a vessel with a volume of 1 litre comprising 1000 g of a water and KOH mixture in which the KOH is present at 75% by weight. HFC-245eb is introduced continuously into the mixture, maintained at 160° C., for 2 hours with a flow rate of 138 g/h and a conversion of HFC-245eb of 83% is obtained for a selectivity for HFO-1234yf of 100%. The pressure is 1 bar.
後処理
- customUse is made of a vessel with a volume of 1 litre
出典と根拠
- ORDレコード
- ord-640a95d50c6446dca2198e9aec32affa
- 出典データセット
- uspto-grants-2016_02
- 特許番号
- US09255047B2
反応ノート
読み込み中…