(4,4-Dimethoxybutyl)(methyl)amine → 2-(5-chloro-1-(2-(3,3-dimethylcyclopentyl)ethyl)-1H-indol-3-yl)-N-methylethanamine

反応式

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]([CH2:10][CH2:11][CH:12]2[CH2:16][CH2:15][C:14]([CH3:18])([CH3:17])[CH2:13]2)N)=[CH:4][CH:3]=1.CO[CH:21](OC)[CH2:22][CH2:23][CH2:24][NH:25][CH3:26]>>[Cl:1][C:2]1[CH:7]=[C:6]2[C:5](=[CH:4][CH:3]=1)[N:8]([CH2:10][CH2:11][CH:12]1[CH2:16][CH2:15][C:14]([CH3:18])([CH3:17])[CH2:13]1)[CH:21]=[C:22]2[CH2:23][CH2:24][NH:25][CH3:26]

参加物

反応物 2

HCID 22563572(4,4-Dimethoxybutyl)(methyl)amine

HCID 669116941-(4-Chlorophenyl)-1-(2-(3,3-dimethylcyclopentyl)ethyl)hydrazine

生成物 1

HCID 669116262-(5-chloro-1-(2-(3,3-dimethylcyclopentyl)ethyl)-1H-indol-3-yl)-N-methylethanamine

実験手順

The title compound is prepared by General Method 10 using 1-(4-chlorophenyl)-1-(2-(3,3-dimethylcyclopentyl)ethyl)hydrazine (Example 5) and 4,4-dimethoxy-N-methylbutan-1-amine.

出典と根拠

ORDレコード: ord-402c59571e0c48d5b06d45c62b601f2e
出典データセット: uspto-grants-2016_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US09260429B2

反応ノート

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